Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200H |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2006-10-17 |
| Detector | RIGAKU-MSC |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 56.385, 86.127, 152.637 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.630 - 1.800 |
| R-factor | 0.15532 |
| Rwork | 0.154 |
| R-free | 0.18722 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1v10 |
| RMSD bond length | 0.032 |
| RMSD bond angle | 2.238 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.630 | 1.847 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.050 | 0.300 |
| Number of reflections | 63965 | |
| <I/σ(I)> | 9.5 | 2.2 |
| Completeness [%] | 96.6 | 90.34 |
| Redundancy | 3.2 | 2.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | PEG 1000, PEG8000., pH 5.5 |
