Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200H |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2006-05-03 |
| Detector | RIGAKU IMAGE PLATE |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 56.020, 85.390, 151.530 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 75.760 - 2.300 |
| R-factor | 0.195 |
| Rwork | 0.193 |
| R-free | 0.22836 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1v10 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.332 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.690 | 2.480 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.110 | 0.470 |
| Number of reflections | 30457 | |
| <I/σ(I)> | 6.5 | 1.6 |
| Completeness [%] | 96.7 | 97.7 |
| Redundancy | 3.5 | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.5 | PEG 1000, PEG 8000, pH 4.5 |
