4A2B
Thermotoga maritima FtsA with ATP gamma S
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-14 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 48.004, 64.594, 73.001 |
Unit cell angles | 90.00, 102.93, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.800 |
R-factor | 0.1783 |
Rwork | 0.176 |
R-free | 0.22257 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1e4f |
RMSD bond length | 0.023 |
RMSD bond angle | 2.400 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.070 | 0.330 |
Number of reflections | 38267 | |
<I/σ(I)> | 10.6 | 3.6 |
Completeness [%] | 99.6 | 99.9 |
Redundancy | 3.5 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.7 | 0.1 M TRIS PH 6.7 42 % ETHANOL |