4A28
Eg5-2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2010-11-18 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.900, 78.390, 92.690 |
Unit cell angles | 90.00, 93.16, 90.00 |
Refinement procedure
Resolution | 29.505 - 2.550 |
R-factor | 0.1842 |
Rwork | 0.180 |
R-free | 0.26370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ii6 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.472 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.690 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.090 | 0.290 |
Number of reflections | 12271 | |
<I/σ(I)> | 10.7 | 5.5 |
Completeness [%] | 98.8 | 97.9 |
Redundancy | 3.5 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | pH 5.5 |