4ZSD

Human Cyclophilin D Complexed with an Inhibitor at room temperature

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM30A
Synchrotron site	ESRF
Beamline	BM30A
Temperature [K]	298
Detector technology	CCD
Collection date	2015-05-07
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9797
Spacegroup name	P 41 21 2
Unit cell lengths	57.943, 57.943, 88.570
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.490 - 1.450
R-factor	0.1349
Rwork	0.134
R-free	0.15540
RMSD bond length	0.008
RMSD bond angle	1.303
Data scaling software	SCALA
Refinement software	REFMAC (5.8.0103)

Data quality characteristics

	Overall
Low resolution limit [Å]	57.940
High resolution limit [Å]	1.450
Number of reflections	25914
<I/σ(I)>	7
Completeness [%]	99.2
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.3	291	30% PEG4000