4ZOY
Crystal structure of the Chaetomium thermophilum Sqt1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-09-27 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.03320 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.440, 73.020, 113.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.377 - 1.500 |
R-factor | 0.1846 |
Rwork | 0.184 |
R-free | 0.20190 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.092 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1685) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 37.380 |
High resolution limit [Å] | 1.500 |
Number of reflections | 89196 |
<I/σ(I)> | 11.2 |
Completeness [%] | 98.7 |
Redundancy | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M Tris pH 8.5, 20% (v/v) EtOH |