4ZOV
Crystal structure of the Saccharomyces cerevisiae Sqt1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-12 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.87260 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.793, 75.165, 101.254 |
Unit cell angles | 90.00, 104.42, 90.00 |
Refinement procedure
Resolution | 42.565 - 2.000 |
R-factor | 0.1882 |
Rwork | 0.187 |
R-free | 0.22290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.210 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1685) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 42.570 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.036 |
Number of reflections | 51857 |
<I/σ(I)> | 16.5 |
Completeness [%] | 98.5 |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 95 mM Na-citrate pH 5.6, 19% (v/v) isopropanol, 19% (w/v) PEG4000, 5% glycerol |