4ZN1
Crystal Structure of MjSpt4:Spt5 complex conformation A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-05-20 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.000 |
Spacegroup name | P 4 |
Unit cell lengths | 84.820, 84.820, 34.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.930 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.299 | |
Number of reflections | 6086 | |
<I/σ(I)> | 20.6 | 3.7 |
Completeness [%] | 99.6 | 99.9 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | PEG 5000MME, propanol, MES, sarcosine |