4ZGO
Structure of C-terminally truncated Cdc123 from Schizosaccharomyces pombe
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-07-03 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 85.600, 91.710, 86.240 |
Unit cell angles | 90.00, 93.53, 90.00 |
Refinement procedure
Resolution | 45.800 - 2.063 |
R-factor | 0.1952 |
Rwork | 0.193 |
R-free | 0.22960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | low-resolution model from SAD experiments |
RMSD bond length | 0.008 |
RMSD bond angle | 1.093 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.800 | 2.190 |
High resolution limit [Å] | 2.060 | 2.060 |
Rmerge | 0.908 | |
Number of reflections | 41180 | |
<I/σ(I)> | 15.7 | 1.3 |
Completeness [%] | 99.0 | 94.3 |
Redundancy | 5.5 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 298 | 12% PEG3350, 4% tacsimate |