4Z9C
EcPltAB Oxidized
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-03-05 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95370 |
Spacegroup name | P 65 |
Unit cell lengths | 160.900, 160.900, 62.640 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.312 - 2.350 |
R-factor | 0.1951 |
Rwork | 0.192 |
R-free | 0.25500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3dwa |
RMSD bond length | 0.011 |
RMSD bond angle | 1.372 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.420 | 2.480 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.041 | 0.356 |
Number of reflections | 38825 | |
<I/σ(I)> | 12.1 | 2.1 |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 8.4 | 8.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 0.2 M magnesium chloride, 0.1 M Tris-HCl, pH 8.5, 15% w/v PEG3350 |