4Z69
Human serum albumin complexed with palmitic acid and diclofenac
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-22 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 1 |
Unit cell lengths | 38.396, 95.003, 96.339 |
Unit cell angles | 105.00, 101.45, 89.97 |
Refinement procedure
Resolution | 45.817 - 2.187 |
R-factor | 0.2287 |
Rwork | 0.225 |
R-free | 0.29300 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.224 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.6_289) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 45.817 |
High resolution limit [Å] | 2.187 |
<I/σ(I)> | 2.1 |
Completeness [%] | 98.0 |
Redundancy | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 285 | PEG 3350, potassium phosphate, glycerol, DMSO |