4Z3U
PRV nuclear egress complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-06-13 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979200 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 125.456, 125.456, 109.235 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.907 - 2.706 |
R-factor | 0.2171 |
Rwork | 0.212 |
R-free | 0.27250 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.787 |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.907 | 2.802 |
High resolution limit [Å] | 2.706 | 2.706 |
Rmerge | 0.087 | 0.617 |
Number of reflections | 24223 | |
<I/σ(I)> | 10.41 | 2.02 |
Completeness [%] | 99.4 | 96 |
Redundancy | 4.55 | 4.21 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.3 M NaSCN, 18% PEG3350, 0.3 M NaCl |