4YYA
The structure of hemagglutinin from a H6N1 influenza virus (A/Taiwan/2/2013) in complex with avian receptor analog 3'SLNLN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-09-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.07138 |
Spacegroup name | P 63 |
Unit cell lengths | 114.194, 114.194, 164.962 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.946 - 2.595 |
R-factor | 0.1834 |
Rwork | 0.182 |
R-free | 0.20820 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.037 |
Data reduction software | SCALA |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.3_1479) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.690 |
High resolution limit [Å] | 2.595 | 2.600 |
Rmerge | 0.126 | 0.494 |
Number of reflections | 37568 | |
<I/σ(I)> | 22 | 6.8 |
Completeness [%] | 99.9 | 100 |
Redundancy | 13.1 | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 0.2M ammonium acetate, 0.1M sodium acetate pH4.0, 15%(w/v) PEG4000 |