4YP9
Crystal Structure of LuxP In Complex With a Formose Derived AI-2 Analogue
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-04-09 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.97618 |
| Spacegroup name | P 43 |
| Unit cell lengths | 104.732, 104.732, 69.532 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.800 - 2.700 |
| R-factor | 0.1694 |
| Rwork | 0.167 |
| R-free | 0.21850 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1jx6 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.062 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.800 | 2.800 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmerge | 0.172 | 0.532 |
| Number of reflections | 20731 | |
| <I/σ(I)> | 7.26 | 2.1 |
| Completeness [%] | 99.2 | 96.5 |
| Redundancy | 3.7 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | MgAc, PEG 8000, sodium cacodylate |
