4YKD
Crystal structure of truncated cerebral cavernous malformation 2 C-terminal adaptor domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-07 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.97908 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 51.360, 51.360, 137.010 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.864 - 1.932 |
R-factor | 0.2021 |
Rwork | 0.200 |
R-free | 0.23460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ykc |
RMSD bond length | 0.014 |
RMSD bond angle | 1.406 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.310 | 2.040 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.079 | |
Number of reflections | 8320 | |
<I/σ(I)> | 55.5 | 30.5 |
Completeness [%] | 97.3 | 96.7 |
Redundancy | 21.1 | 21.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.1 M Bis-Tris, 30%(w/v) polyethylene glycol 550, 50 mM calcium chloride |