4YH2
Glutathione Transferase E6 from Drosophila melanogaster
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-09-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.976 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 176.350, 58.860, 122.810 |
Unit cell angles | 90.00, 128.25, 90.00 |
Refinement procedure
Resolution | 96.440 - 1.720 |
R-factor | 0.1587 |
Rwork | 0.157 |
R-free | 0.18840 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.057 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | xia2 |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 96.440 |
High resolution limit [Å] | 1.720 |
Number of reflections | 105003 |
<I/σ(I)> | 12.3 |
Completeness [%] | 99.8 |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 288 | PEG3350, Sodium thiocyanate |