4YFO
beta1_ex1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-05-26 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.92000 |
Spacegroup name | H 3 2 |
Unit cell lengths | 105.180, 105.180, 323.500 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.680 - 3.390 |
R-factor | 0.19733 |
Rwork | 0.196 |
R-free | 0.23339 |
RMSD bond length | 0.022 |
RMSD bond angle | 2.522 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 107.830 | 3.480 |
High resolution limit [Å] | 3.390 | 3.390 |
Rmerge | 0.129 | 0.585 |
Number of reflections | 9607 | |
<I/σ(I)> | 14.3 | 4.3 |
Completeness [%] | 96.8 | 98.9 |
Redundancy | 9.9 | 9.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 291 | 90 mM Bis Tris pH 5.5, 2.7 M sodium chloride |