Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-10-02 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.9801 |
| Spacegroup name | P 1 |
| Unit cell lengths | 63.620, 68.480, 87.070 |
| Unit cell angles | 109.38, 92.66, 117.66 |
Refinement procedure
| Resolution | 49.380 - 2.330 |
| R-factor | 0.20479 |
| Rwork | 0.202 |
| R-free | 0.25265 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2ivp |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.662 |
| Data reduction software | XDS |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0071) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.380 | 2.330 |
| High resolution limit [Å] | 2.250 | 2.250 |
| Rmerge | 0.570 | |
| Number of reflections | 55653 | |
| <I/σ(I)> | 11 | 2.46 |
| Completeness [%] | 97.9 | 95.69 |
| Redundancy | 3.97 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 293 | 30% PEG4000, 0.3M Lithium Sulfate, 0.1 M Sodium Acetate and 0.1 M HEPES |
