4Y9V
Gp54 tailspike of Acinetobacter baumannii bacteriophage AP22 in complex with A. baumannii capsular saccharide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-05 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.8 |
Spacegroup name | H 3 2 |
Unit cell lengths | 92.634, 92.634, 391.478 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.900 - 0.900 |
R-factor | 0.0972 |
Rwork | 0.097 |
R-free | 0.10920 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 0.030 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | SHELXL |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.900 | 0.960 |
High resolution limit [Å] | 0.900 | 0.900 |
Rmerge | 0.073 | 0.353 |
Number of reflections | 466729 | |
<I/σ(I)> | 13.7 | 3 |
Completeness [%] | 97.7 | 86.3 |
Redundancy | 4.5 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.1 | 293 | 6-10% PEG8000, 500mM Li2SO4, 100mM MES pH 6.5 |