4Y7A

Factor Xa complex with GTC000422

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX9.6
Synchrotron site	SRS
Beamline	PX9.6
Temperature [K]	100
Detector technology	CCD
Collection date	2001-03-28
Detector	ADSC QUANTUM 4
Spacegroup name	P 21 21 21
Unit cell lengths	57.160, 73.477, 80.377
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 1.990
R-factor	0.1913
Rwork	0.189
R-free	0.23620
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1ezq
RMSD bond length	0.010
RMSD bond angle	1.349
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.6.0117)

Data quality characteristics

	Overall
Low resolution limit [Å]	26.630
High resolution limit [Å]	1.990
Rmerge	0.085
Number of reflections	23605
<I/σ(I)>	11.8
Completeness [%]	99.3
Redundancy	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	18% PEG 6000, 100 mM MES PH 5.75, 10 mM calcium chloride