4Y0N
SAV1875
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 6C1 |
| Synchrotron site | PAL/PLS |
| Beamline | 6C1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-08-27 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 1.23986 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 81.455, 95.004, 42.648 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 37.780 - 2.100 |
| R-factor | 0.19291 |
| Rwork | 0.191 |
| R-free | 0.22649 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1oi4 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.052 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.000 |
| High resolution limit [Å] | 2.100 |
| Number of reflections | 19995 |
| <I/σ(I)> | 39.2 |
| Completeness [%] | 99.5 |
| Redundancy | 6.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 29% PEG mme2000, 100mM Bis-Tris |
