Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-08-26 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.979740 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 131.443, 205.298, 234.410 |
Unit cell angles | 90.00, 94.10, 90.00 |
Refinement procedure
Resolution | 48.828 - 3.796 |
R-factor | 0.2862 |
Rwork | 0.285 |
R-free | 0.29940 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 1.241 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.830 | 3.860 |
High resolution limit [Å] | 3.790 | 3.790 |
Rmerge | 0.383 | 3.826 |
Number of reflections | 243648 | |
<I/σ(I)> | 8.8 | 0.9 |
Completeness [%] | 99.3 | 87.5 |
Redundancy | 20 | 16.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M CHES, pH 9.2, 29% v/v PEG400 |