4XOD
Crystal structure of a FimH*DsG complex from E.coli F18
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-02-11 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.99999 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 99.310, 35.540, 72.790 |
Unit cell angles | 90.00, 105.80, 90.00 |
Refinement procedure
Resolution | 47.779 - 1.140 |
R-factor | 0.1428 |
Rwork | 0.142 |
R-free | 0.15850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3mcy 1qun |
RMSD bond length | 0.006 |
RMSD bond angle | 1.166 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: dev_1621)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.779 | 1.210 |
High resolution limit [Å] | 1.140 | 1.140 |
Rmerge | 0.033 | 0.610 |
Number of reflections | 87277 | |
<I/σ(I)> | 16.6 | 1.6 |
Completeness [%] | 97.4 | 88 |
Redundancy | 3.1 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 277 | 25 % (w/v) PEG 3350, 0.2 M magnesium chloride, 0.1 M BisTris-HCl pH 5.5 |