4XN6
Crystal structure at room temperature of hen-egg lysozyme in complex with benzamidine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2014-07-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9797 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.292, 79.292, 38.073 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.100 - 1.350 |
R-factor | 0.1397 |
Rwork | 0.138 |
R-free | 0.16550 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.239 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 38.100 |
High resolution limit [Å] | 1.350 |
Number of reflections | 21988 |
<I/σ(I)> | 2.5 |
Completeness [%] | 99.5 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 298 | NaOAc 100mM ,4% (w/v) NaCl |