4XGQ

Crystal structure of addiction module from Mycobacterial species

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	CCD
Collection date	2013-09-11
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0000
Spacegroup name	P 31 2 1
Unit cell lengths	96.381, 96.381, 232.788
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	40.660 - 2.700
R-factor	0.20736
Rwork	0.206
R-free	0.23814
RMSD bond length	0.011
RMSD bond angle	1.212
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	REFMAC (5.7.0032)

Data quality characteristics

	Overall
Low resolution limit [Å]	40.660
High resolution limit [Å]	2.700
Number of reflections	35181
<I/σ(I)>	40.96
Completeness [%]	99.3
Redundancy	7.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.1M sodium citrate tribasic dihydrate pH 5.6, 1.0M ammonium phosphate monobasic