4X2M
Structure of Mtr2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-11-05 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9686 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 83.958, 83.958, 131.340 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.819 - 2.000 |
R-factor | 0.1818 |
Rwork | 0.181 |
R-free | 0.20180 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.716 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 38.827 |
High resolution limit [Å] | 2.000 |
Number of reflections | 31939 |
<I/σ(I)> | 12.2 |
Completeness [%] | 98.7 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 1.26 M Ammonium Sulphate, 0.1 M MES pH 6.0. See publication for details. |