4X06
Crystal structure of P domain from norovirus strain Saga4 in complex with HBGA type B (triglycan)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97248 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 113.830, 58.650, 97.310 |
Unit cell angles | 90.00, 107.34, 90.00 |
Refinement procedure
Resolution | 32.323 - 1.218 |
R-factor | 0.1354 |
Rwork | 0.134 |
R-free | 0.16120 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.357 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.3) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 1.250 | ||
High resolution limit [Å] | 1.220 | 5.450 | 1.220 |
Rmerge | 0.035 | 0.031 | 0.354 |
Rmeas | 0.043 | 0.039 | 0.442 |
Total number of observations | 457076 | ||
Number of reflections | 176472 | 2040 | 12148 |
<I/σ(I)> | 13.92 | 34.3 | 2.54 |
Completeness [%] | 96.7 | 94.7 | 90.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.9 | 291 | Sodium acetate |