4WSR
The crystal structure of hemagglutinin form A/chicken/New York/14677-13/1998
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-03-20 |
| Detector | MARMOSAIC 325 mm CCD |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 252.545, 134.822, 123.093 |
| Unit cell angles | 90.00, 113.23, 90.00 |
Refinement procedure
| Resolution | 48.000 - 2.500 |
| R-factor | 0.21176 |
| Rwork | 0.210 |
| R-free | 0.24617 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.601 |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 48.000 |
| High resolution limit [Å] | 2.500 |
| Number of reflections | 129493 |
| <I/σ(I)> | 30.6 |
| Completeness [%] | 99.0 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 293 | 0.2 M ammonium fluoride, 20% (w/v) PEG 3350 |
