4WPX
Chaetomium theromophilum TREX2 CID domain complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-06-30 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.9700 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 56.528, 168.288, 69.223 |
| Unit cell angles | 90.00, 112.21, 90.00 |
Refinement procedure
| Resolution | 19.904 - 3.310 |
| R-factor | 0.2207 |
| Rwork | 0.218 |
| R-free | 0.27660 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.792 |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.904 |
| High resolution limit [Å] | 3.310 |
| Number of reflections | 17487 |
| <I/σ(I)> | 6.9 |
| Completeness [%] | 98.0 |
| Redundancy | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | see publication for details |
