4WP6

Structure of the Mex67 LRR domain from Chaetomium thermophilum

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	CCD
Collection date	2011-12-09
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9795
Spacegroup name	C 1 2 1
Unit cell lengths	113.817, 33.100, 43.495
Unit cell angles	90.00, 91.65, 90.00

Refinement procedure

Resolution	43.477 - 1.700
R-factor	0.1873
Rwork	0.185
R-free	0.21330
RMSD bond length	0.008
RMSD bond angle	1.021
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	43.500
High resolution limit [Å]	1.700
Number of reflections	18096
<I/σ(I)>	9.5
Completeness [%]	99.8
Redundancy	4.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	see publication for details