4WO6

Lysozyme Pre-surface acoustic wave

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CHESS BEAMLINE A1
Synchrotron site	CHESS
Beamline	A1
Temperature [K]	100
Detector technology	CCD
Collection date	2014-03-30
Detector	ADSC QUANTUM 210
Wavelength(s)	0.978
Spacegroup name	P 43 21 2
Unit cell lengths	79.349, 79.349, 37.597
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.054 - 2.001
R-factor	0.1592
Rwork	0.154
R-free	0.20920
RMSD bond length	0.007
RMSD bond angle	1.034
Data reduction software	HKL-2000
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.000
Number of reflections	64483
<I/σ(I)>	16.8
Completeness [%]	100.0
Redundancy	7.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	BATCH MODE	4.6	277	1 M NaCl, 25% Glycerol, 0.1 M Na Acetate, pH 4.6, gentle agitation