4WJA
Crystal Structure of PAXX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-22 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 91.825, 91.825, 152.468 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.475 - 2.600 |
R-factor | 0.2473 |
Rwork | 0.245 |
R-free | 0.26650 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.566 |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 79.523 |
High resolution limit [Å] | 2.600 |
Number of reflections | 12287 |
<I/σ(I)> | 69.64 |
Completeness [%] | 99.3 |
Redundancy | 20 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289 | 2.24M Ammonium sulfate, 0.1M Bis-Tris, pH 5.5 |