4WE8

The crystal structure of hemagglutinin of influenza virus A/Victoria/361/2011

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-ID
Synchrotron site	APS
Beamline	22-ID
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2013-03-16
Detector	MAR scanner 345 mm plate
Wavelength(s)	1.0
Spacegroup name	H 3 2
Unit cell lengths	100.911, 100.911, 383.361
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	34.156 - 2.100
R-factor	0.1923
Rwork	0.190
R-free	0.22730
RMSD bond length	0.005
RMSD bond angle	0.931
Refinement software	PHENIX ((phenix.refine: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.100
Number of reflections	43789
<I/σ(I)>	37.1
Completeness [%]	98.5
Redundancy	5.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	MICROBATCH	10.5	293	0.1M CAPS:NaOH, 30% PEG 400