4WBF
Acinetobacter baumannii SDF NDK
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 180 |
Detector technology | CCD |
Collection date | 2014-09-01 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5419 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 60.330, 75.400, 82.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.107 - 2.640 |
R-factor | 0.2068 |
Rwork | 0.201 |
R-free | 0.25810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4w98 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.102 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.110 |
High resolution limit [Å] | 2.490 |
Number of reflections | 6880 |
<I/σ(I)> | 7.3 |
Completeness [%] | 100.0 |
Redundancy | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 289 | Sodium malonate, HEPES, Jeffamine ED-2001 |