Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 90 |
| Detector technology | PIXEL |
| Collection date | 2009-11-16 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.999 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 437.110, 288.380, 306.560 |
| Unit cell angles | 90.00, 99.13, 90.00 |
Refinement procedure
| Resolution | 268.000 - 4.000 |
| R-factor | 0.28 |
| Rwork | 0.278 |
| R-free | 0.34100 |
| Structure solution method | molecular replacement + SAD |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 268.000 | 4.350 | 4.150 |
| High resolution limit [Å] | 4.000 | 4.150 | 4.000 |
| Number of reflections | 619044 | ||
| <I/σ(I)> | 2 | 1 | |
| Completeness [%] | 98.1 | 97.9 | 84.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | 297 | PEG 20K, KSCN, Mg Acetate, Tris-Acetate, Glycerol, Spermidine, pH 7, VAPOR DIFFUSION, temperature 297K |
