4V5B
Structure of PDF binding helix in complex with the ribosome.
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-02-21 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 208.181, 380.083, 736.701 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 3.740 |
Rwork | 0.259 |
R-free | 0.32300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2AW4 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.740 |
Rmerge | 0.180 |
Number of reflections | 546832 |
<I/σ(I)> | 5.1 |
Completeness [%] | 91.5 |
Redundancy | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |