4UV6
Crystal structure of apical membrane antigen 1 from Plasmodium knowlesi
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-11-05 |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 90.320, 105.700, 104.750 |
| Unit cell angles | 90.00, 98.04, 90.00 |
Refinement procedure
| Resolution | 47.090 - 2.450 |
| R-factor | 0.172 |
| Rwork | 0.171 |
| R-free | 0.22660 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1w81 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.150 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.4) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.090 | 2.580 |
| High resolution limit [Å] | 2.450 | 2.450 |
| Rmerge | 0.100 | 0.500 |
| Number of reflections | 34848 | |
| <I/σ(I)> | 9.7 | 1.9 |
| Completeness [%] | 97.3 | 93.3 |
| Redundancy | 2.9 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8.4 | 0.86M SODIUM CITRATE, 0.1M HEPES PH 8.4 |
