4UNW

Structure of the A_Equine_Newmarket_2_93 H3 haemagglutinin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I02
Synchrotron site	Diamond
Beamline	I02
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 21 21 21
Unit cell lengths	100.679, 102.506, 229.489
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	114.740 - 2.600
R-factor	0.18789
Rwork	0.186
R-free	0.22835
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3ztj
RMSD bond length	0.008
RMSD bond angle	1.376
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	REFMAC (5.8.0069)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.170	2.740
High resolution limit [Å]	2.600	2.600
Rmerge	0.070	0.540
Number of reflections	73772
<I/σ(I)>	18.5	3.6
Completeness [%]	99.9	99.9
Redundancy	6.7	6.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1