4UB6
Native structure of photosystem II (dataset-1) by a femtosecond X-ray laser
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | SACLA BEAMLINE BL3 |
| Synchrotron site | SACLA |
| Beamline | BL3 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-03-16 |
| Detector | RAYONIX MX225HE |
| Wavelength(s) | 1.24 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 123.744, 229.989, 288.337 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 62.287 - 1.950 |
| R-factor | 0.1995 |
| Rwork | 0.198 |
| R-free | 0.23820 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.442 |
| Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 62.700 |
| High resolution limit [Å] | 1.950 |
| Number of reflections | 585462 |
| <I/σ(I)> | 3.5 |
| Completeness [%] | 98.7 |
| Redundancy | 4.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 290 | PEG, magnesium sulfate |
