4U9R
Structure of the N-terminal Extension from Cupriavidus metallidurans CzcP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-07-16 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.03322 |
Spacegroup name | P 41 |
Unit cell lengths | 58.160, 58.160, 72.010 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.010 - 2.170 |
R-factor | 0.2313 |
Rwork | 0.228 |
R-free | 0.26610 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.465 |
Data scaling software | xia2 |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 36.010 | 36.010 | 2.230 |
High resolution limit [Å] | 2.170 | 9.710 | 2.170 |
Rmerge | 0.053 | 0.024 | 0.719 |
Rpim | 0.016 | 0.007 | 0.223 |
Total number of observations | 144365 | 1598 | 10281 |
Number of reflections | 12757 | ||
<I/σ(I)> | 26.8 | 80.2 | 4 |
Completeness [%] | 99.8 | 97.4 | 99.7 |
Redundancy | 11.3 | 10.7 | 11.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 298 | PEG 4000, 1 mM CdSO4 |