4U76
HsMetAP (F309M) holo form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2014-02-27 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 47.067, 77.469, 46.990 |
| Unit cell angles | 90.00, 92.43, 90.00 |
Refinement procedure
| Resolution | 18.720 - 1.870 |
| R-factor | 0.18 |
| Rwork | 0.177 |
| R-free | 0.22300 |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.953 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 1.870 |
| Number of reflections | 26625 |
| <I/σ(I)> | 3.1 |
| Completeness [%] | 99.6 |
| Redundancy | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 15% PEGMME, 100mM HEPES PH 6 |
