4U6J
HsMetAP in complex with methionine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2014-03-11 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 47.446, 77.340, 48.440 |
| Unit cell angles | 90.00, 90.93, 90.00 |
Refinement procedure
| Resolution | 18.530 - 1.560 |
| R-factor | 0.127 |
| Rwork | 0.125 |
| R-free | 0.17600 |
| RMSD bond length | 0.021 |
| RMSD bond angle | 2.057 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 18.930 |
| High resolution limit [Å] | 1.560 |
| Number of reflections | 48263 |
| <I/σ(I)> | 4.8 |
| Completeness [%] | 97.0 |
| Redundancy | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 15% PEG MME , 100mM HEPES PH6.0 , |
