4TZN

Structure of HTP-2 bound to HTP-3 motif-6

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-E
Synchrotron site	APS
Beamline	24-ID-E
Temperature [K]	100
Detector technology	CCD
Collection date	2013-11-09
Detector	ADSC QUANTUM 315
Wavelength(s)	.979
Spacegroup name	C 1 2 1
Unit cell lengths	165.820, 38.310, 103.820
Unit cell angles	90.00, 126.24, 90.00

Refinement procedure

Resolution	80.000 - 3.115
R-factor	0.282
Rwork	0.280
R-free	0.31980
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4tzl
RMSD bond length	0.003
RMSD bond angle	0.604
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	80.000
High resolution limit [Å]	3.100
Number of reflections	8218
<I/σ(I)>	8.7
Completeness [%]	83.4
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	298.15	15-22% PEG 3350