4TWL
Crystal structure of dioscorin complexed with ascorbate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 95 |
| Detector technology | CCD |
| Collection date | 2011-02-27 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.0000 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 83.505, 157.103, 83.485 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.110 |
| R-factor | 0.20476 |
| Rwork | 0.201 |
| R-free | 0.26604 |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.941 |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.110 |
| Number of reflections | 31531 |
| <I/σ(I)> | 51.6 |
| Completeness [%] | 99.0 |
| Redundancy | 6.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 9 | 278 | BICINE, PEG400, ammonium sulfate |
