4TUG
Crystal structure of MjMre11-DNA2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 103 |
Detector technology | CCD |
Collection date | 2011-06-23 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 91.530, 185.624, 106.212 |
Unit cell angles | 90.00, 99.86, 90.00 |
Refinement procedure
Resolution | 42.422 - 3.550 |
R-factor | 0.1868 |
Rwork | 0.184 |
R-free | 0.23580 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.163 |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.550 |
Number of reflections | 41919 |
<I/σ(I)> | 13.3 |
Completeness [%] | 100.0 |
Redundancy | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | PEG |