4TT0

Crystal structure of fragment 1600-1733 of HSV1 UL36 in the presence of 1M potassium iodide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-1
Synchrotron site	ESRF
Beamline	ID23-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2012-11-11
Detector	PSI PILATUS 6M
Wavelength(s)	1.907450
Spacegroup name	P 61 2 2
Unit cell lengths	110.939, 110.939, 154.930
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	48.038 - 2.599
R-factor	0.1905
Rwork	0.188
R-free	0.24200
Structure solution method	SAD
RMSD bond length	0.008
RMSD bond angle	1.031
Data reduction software	XDS
Phasing software	SHELXDE
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	48.038
High resolution limit [Å]	2.599
Number of reflections	32816
<I/σ(I)>	14.5
Completeness [%]	100.0
Redundancy	6.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	293	100 mM Hepes, 2M ammonium formate