Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.2 |
| Synchrotron site | ALS |
| Beamline | 8.2.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-06-14 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.48690 |
| Spacegroup name | P 32 |
| Unit cell lengths | 33.110, 33.110, 154.281 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 51.427 - 2.285 |
| R-factor | 0.2302 |
| Rwork | 0.223 |
| R-free | 0.29900 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.274 |
| Refinement software | PHENIX ((phenix.refine: dev_1420)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 51.430 |
| High resolution limit [Å] | 2.280 |
| Number of reflections | 7223 |
| <I/σ(I)> | 11.6 |
| Completeness [%] | 83.6 |
| Redundancy | 5.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 296 | 0.1M BIS-TRIS, 10MM NICKEL (II) CHLORIDE, 10MM CESIUM CHLORIDE, 20% PEG MME 2000 |
