4RM0

Crystal structure of Norovirus OIF P domain in complex with Lewis a trisaccharide

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	CCD
Detector	RIGAKU SATURN 944
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	54.851, 84.158, 124.742
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	25.055 - 1.999
R-factor	0.1728
Rwork	0.171
R-free	0.20930
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.097
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.7_650))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.070
High resolution limit [Å]	1.999	2.000
Rmerge		0.236
Number of reflections	37781
<I/σ(I)>		3.7
Completeness [%]	94.7	68.4
Redundancy		2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1