4RCX
Trichomonas vaginalis triosephosphate isomerase TVAG_497370 gene (Ile-45 variant) loop 3 deletion protein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-08-15 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.98 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 46.970, 56.730, 105.860 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.960 - 1.750 |
R-factor | 0.1747 |
Rwork | 0.173 |
R-free | 0.20290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.016 |
RMSD bond angle | 1.626 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: dev_1730)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 29.963 |
High resolution limit [Å] | 1.750 |
Rmerge | 0.065 |
Number of reflections | 29120 |
<I/σ(I)> | 11.2 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 294 | 0.2 M Calcium acetate, 0.1 M Sodium cacodylate, 18 % PEG 8000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |