4RB3
Crystal structure of Magnetospirillum gryphiswaldense MSR-1 Fur-Mn2+-feoAB1 operator
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BSRF BEAMLINE 3W1A |
| Synchrotron site | BSRF |
| Beamline | 3W1A |
| Temperature [K] | 130 |
| Detector technology | CCD |
| Collection date | 2012-12-26 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 93.995, 68.642, 83.995 |
| Unit cell angles | 90.00, 108.70, 90.00 |
Refinement procedure
| Resolution | 44.560 - 2.600 |
| R-factor | 0.23411 |
| Rwork | 0.232 |
| R-free | 0.26485 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4rb2 |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.944 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.640 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Number of reflections | 15330 | |
| Completeness [%] | 97.1 | 85.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
